The overall procedure of X-ray fluorescence analysis may be divided into three different stages: sampling, sample preparation and the actual spectrometric analysis itself. Of these three, it is usually the mechanical sample preparation that takes up most of the time and will therefore be discussed in this application report.
Quality control is an important aspect of cement production. Sample preparation is an essential part of it, because only a representative and reproducible processing of the sample material ensures reliable and meaningful analysis results. RETSCH offers a range of instruments for dividing, crushing, grinding and sizing all materials which are involved in the production process of cement, including secondary fuels. To ensure the right choice of instrument for the right sample material, Retsch offers free-of-charge sample testing in application laboratories all over the world.
Reliable and accurate analysis results can only be guaranteed by reproducible sample preparation. This consists of transforming a laboratory sample into a representative part sample with homogeneous analytical fineness. Retsch offers a comprehensive range of the most modern mills and crushers for coarse, fine and ultra-fine size reduction of almost any material. The product range also comprises a wide choice of grinding tools and accessories which helps to ensure contamination-free preparation of a great variety of sample materials. The selection of the correct grinding tool depends on the sample material and the subsequent method of analysis. Different grinding tools have different characteristics, such as required energy input, hardness or wear-resistance.
A variety of methods can be used to analyze solid materials. What they all have in common is the necessity to use a representative, homogeneous analysis sample which needs to have a particular fineness, depending on the analytical method used. The size reduction and homogenization of solids is usually carried out with laboratory crushers and grinders.
A faultless and comparable analysis is closely linked to an accurate sample handling. Only a sample representative of the initial material can provide meaningful analysis results. Rotating dividers and rotary tube dividers are an important means to ensure the representativeness of a sample and thus the reproducibility of the analysis. Correct sample handling consequently minimizes the probability of a production stop due to incorrect analysis results. Thus correct sample handling is the key to effective quality control.
The preparation of a mixture of organic and inorganic samples holds some difficulties: whereas sand, clay and stones can usually be ground to homogeneous samples with suitable laboratory mills, the high energy input can cause samples with organic components such as fat or starch to cake. Carsten Bunn, a laboratory technician at the waste water treatment laboratory BRW, has to deal with this problem every day. He treats samples which are taken from the sand traps of the wastewater treatment plants and consist of exactly that mixture. The sediments of household and industry waste water not only contain sand, clay or leaves but anything that people nowadays dispose of through the sewer system: cellulose, hair and especially food residues.
To produce high-quality cement, the mineralogical and chemical composition of raw materials as well as intermediate and finished products has to be determined. At each stage of the production, samples have to be taken, processed and analysed to ensure quality control without gaps. Retsch offers a range of instruments that are used for sample preparation during the complete production process, from the quarrying of the raw materials to the final product. The typical sample preparation process involves preliminary size reduction, sample division and fine size reduction before the sample can be submitted to further analyses....
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How to get the best results with the Vibratory Disc Mill RS 200
Why Size Reduction? A reliable and accurate analysis can only be guaranteed by reproducible sample preparation. The "Art of Milling" describes the process of turning a laboratory sample into a representative part sample with homogeneous analytical fineness.